Instructions

Beginners

Reference Tables

DPX 200

Avance 300

Avance III 400

Avance 500

Avance III 600

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Listing By Experiment:

• 1D 1H NMR, AV 300 and AV500, Topspin version 2.1
  or pocketmod, Topspin version 2.1
  or DPX 200, Topspin version 1.3
• 1D X NMR (not 1H):
  (13C, 31P, 19F) DPX200
  (29Si, 13C, 31P) AV300
  Common carbon experiments
• 2D NMR
• Automatic shut-down of Topspin
• Calibration, chemical shift
• COSY, 1D selective
• Deuterium NMR
• DOSY, Self-diffusion coefficients
• Homonuclear decoupling, 1H
• Inverse gated decoupling (zgig)
• Janocchio
• Kinetics analysis via pseudo-2D NMR
• 15N NMR
• NOE, 1D selective (best with gradients)
• NOE, 1D difference spectroscopy
• Pulse calibrations
• Quantitative NMR
• Quantification of an unknown concentration
• Saturation transfer (STD)
• Solvent suppression
  watergate 3919, with gradients
  Wet multiple-frequency, with gradients
  no gradients: noesypr1d
• Sum blocks of data
• T1 inversion-recovery
• T2 Measurements (solids)
• TOCSY, 1D selective with gradients
• Variable temperature NMR (*calibration)
• Variable temperature, automated cool-down: multi_zgvt (solids 47Ti example)
• XWIN-PLOT